HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium → HCID 21270775, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 21270720 | HCID 21270720 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 21270775 | HCID 21270775 | — |
Reaction Steps
using 2-chloro-1-(4-chloro-2-fluoro-5-isopropoxyphenyl)-4-pentafluoroethyl-6(1H)-pyrimidinone and sodium isopropylate in isopropanol there is obtained 1-(4-chloro-2-fluoro-5-isopropoxyphenyl)-2-isopropoxy-4-pentafluoroethyl-6(1H)-pyrimidinone, 1H-NMR (CDCl3, 400 MHz): 7.30 ppm (d,1H), 6.81 ppm (d,1H), 6.62 ppm (s,1H), 5.33 ppm (m,1H), 4.47 ppm (m,1H), 1.38 ppm (d,3H), 1.37 ppm (d,3H), 1.28 ppm (d,3H), 1.27 ppm (d,3H);
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04812164 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-ee4d471f7bb94329b88e0827b8e2be07 |
| Source note | uspto-grants-1989_03 |