HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium → HCID 21270713, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 21270720 | HCID 21270720 | — |
| Solvent | 1-Propanol | HCID 1031 | — |
| Product | HCID 21270713 | HCID 21270713 | — |
Reaction Steps
using 2-chloro-1-(4-chloro-2-fluoro-5-isopropoxyphenyl)-4-pentafluoroethyl-6(1H)-pyrimidinone and sodium propylate in n-propanol there is obtained 1-(4-chloro-2-fluoro-5-isopropoxyphenyl)-4 -pentafluoroethyl-2-(n-propoxy)-6(1H)-pyrimidinone, 1H-NMR (CDCl3, 400 MHz): 7.31 ppm (d,1H), 6.82 ppm (d,1H), 6.63 ppm (s,1H), 4.46 ppm (m,1H), 4.36 ppm (m,2H), 1.66 ppm (m,2H), 1.38 ppm (d,3H), 1.37 ppm (d,3H), o.85 ppm (t,3H);
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04812164 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-77efb9a5970646ff9b0da878c971d362 |
| Source note | uspto-grants-1989_03 |