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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1193889Generated: November 1, 2026

Dimethyl Sulfate → HCID 21270752, compound

https://huagongshe.com/reaction/1193889

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethyl SulfateHCID 6497—
ReactantSodium BicarbonateHCID 516892—
ReactantHCID 21270777HCID 21270777—
SolventAcetoneHCID 180—
ProductHCID 21270752HCID 21270752—

Reaction Steps

using 3-(4-chloro-3-isopropoxyphenyl)-6-trifluoromethyl-2,4(1H,3H)-pyrimidinedione with dimethyl sulphate and sodium bicarbonate in acetone there is obtained 1-(4-chloro-3-isopropoxyphenyl)-2-methoxy-4-trifluoromethyl -6(1H)-pyrimidinone. m.p. 55°-58° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04812164
Source datasetuspto-grants-1989_03
ORD IDord-c96330bfabd341bab5484eb620e6265d
Source noteuspto-grants-1989_03