HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → HCID 53722627, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | HCID 21270727 | HCID 21270727 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 53722627 | HCID 53722627 | — |
Reaction Steps
using 2-ethoxy-1-(4-chloro-2-fluoro-5 -hydroxyphenyl) -4-trifluoromethyl-6(1H)-pyrimidinone and dimethyl sulphate with sodium carbonate in acetone there is obtained 2-ethoxy-1-(4-chloro-2-fluoro-5 -methoxyphenyl) -4-trifluoromethyl-6(1H)-pyrimidinone. m.p. 117°-119° C.;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04812164 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-30aeec422cc54fac901a0806b42fb1b1 |
| Source note | uspto-grants-1989_03 |