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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1193908Generated: October 31, 2026

Pyridine → HCID 53892817, compound

https://huagongshe.com/reaction/1193908

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPyridineHCID 1049—
Reactant2-Methoxyethyl chloroformateHCID 69400—
ReactantHCID 21270730HCID 21270730—
SolventDiethyl EtherHCID 3283—
ProductHCID 53892817HCID 53892817—

Reaction Steps

using 2-ethoxy-1-(4-chloro-2-fluoro-5-hydroxyphenyl)-4-pentafluoroethyl-6(1H)-pyrimidinone and 2-methoxyethyl chloroformate with pyridine in diethyl ether there is obtained {5-[2-ethoxy-6-oxo-4-pentafluoroethyl-1(6H) -pyrimidinyl]-2-chloro-4-fluorophenyl} 2-methoxyethyl carbonate, 1H-NMR (CDCl3, 400 MHz): 7.39 ppm (d,1H), 7.26 ppm (d,1H), 6.64 ppm (s,1H), 4.39°-4.56 ppm (m,4H), 3.70 ppm (m,2H), 3.43 ppm (s,3H), 1.30 ppm (t,3H):

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04812164
Source datasetuspto-grants-1989_03
ORD IDord-3175c368aa5c4d509deb269ca1a2b15f
Source noteuspto-grants-1989_03