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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1193910Generated: November 1, 2026

Allyl bromide → HCID 21270793, compound

https://huagongshe.com/reaction/1193910

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAllyl bromideHCID 7841—
ReactantSodium hydrideHCID 24758—
ReactantHCID 21270719HCID 21270719—
SolventDimethylformamideHCID 6228—
ProductHCID 21270793HCID 21270793—

Reaction Steps

using 1-(4-bromo-2-fluoro-5-hydroxyphenyl)-2-methoxy-4-trifluoromethyl-6(1H)-pyrimidinone and allyl bromide with sodium hydride in dimethylformamide there is obtained 1-(5-allyloxy-4-bromo-2-fluorophenyl)-2-methoxy-4-trifluoromethyl-6(1H)-pyrimidinone. m.p. 107°-110° C.;

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04812164
Source datasetuspto-grants-1989_03
ORD IDord-96e3f09abea64ac986d9d30ef8740800
Source noteuspto-grants-1989_03