HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propargyl bromide → HCID 21270765, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propargyl bromide | HCID 7842 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 21270719 | HCID 21270719 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 21270765 | HCID 21270765 | — |
Reaction Steps
using 1-(4-bromo-2-fluoro-5-hydroxyphenyl)-2-methoxy-4-trifluoromethyl-6(1H)-pyrimidinone and propargyl bromide with sodium hydride in dimethylformamide there is obtained 1-[4-bromo-2-fluoro-5-(2-propynyloxy)-phenyl]-2-methoxy-4-trifluoromethyl-6(1H)-pyrimidinone, m.p. 136°-138° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04812164 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-423b5a4873974e7abb38a4dbc6c76dec |
| Source note | uspto-grants-1989_03 |