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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1193913Generated: October 29, 2026

Chloromethyl Methyl Ether → HCID 21270703, compound

https://huagongshe.com/reaction/1193913

Reaction equation

Participants

RoleNameHCIDCharge
ReactantChloromethyl Methyl EtherHCID 7864—
ReactantSodium hydrideHCID 24758—
ReactantHCID 21270789HCID 21270789—
SolventDimethylformamideHCID 6228—
ProductHCID 21270703HCID 21270703—

Reaction Steps

using 1-(4-chloro-2-fluoro-5-hydroxyphenyl)-5-fluoro-2-methoxy-4-pentafluoroethyl-6(1H)-pyrimidinone and chlorodimethyl ether with sodium hydride in dimethylformamide there is obtained 1-(4-chloro-2-fluoro-5 -methoxymethoxy-phenyl)-5-fluoro-2-methoxy-4-pentafluoroethyl-6(1H)-pyrimidinone, 1H-NMR CDCl3, 400 MHz): 7.34 ppm (d,1H), 7.13 ppm (d,1H), 5.22 ppm (q,2H), 3.98 ppm (s,3H), 3.52 ppm (s,3H);

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04812164
Source datasetuspto-grants-1989_03
ORD IDord-4d503760ad6040aa931f6f55e4e98b00
Source noteuspto-grants-1989_03