HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloromethyl Methyl Ether → HCID 21270703, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloromethyl Methyl Ether | HCID 7864 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 21270789 | HCID 21270789 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 21270703 | HCID 21270703 | — |
Reaction Steps
using 1-(4-chloro-2-fluoro-5-hydroxyphenyl)-5-fluoro-2-methoxy-4-pentafluoroethyl-6(1H)-pyrimidinone and chlorodimethyl ether with sodium hydride in dimethylformamide there is obtained 1-(4-chloro-2-fluoro-5 -methoxymethoxy-phenyl)-5-fluoro-2-methoxy-4-pentafluoroethyl-6(1H)-pyrimidinone, 1H-NMR CDCl3, 400 MHz): 7.34 ppm (d,1H), 7.13 ppm (d,1H), 5.22 ppm (q,2H), 3.98 ppm (s,3H), 3.52 ppm (s,3H);
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04812164 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-4d503760ad6040aa931f6f55e4e98b00 |
| Source note | uspto-grants-1989_03 |