HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → 2-Dimethylaminopyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Catalyst | Triethylamine | HCID 8471 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 2-Dimethylaminopyridine | HCID 21885 | — |
Reaction Steps
This condensation is carried out in solution either in dimethylformamide using triethylamine as catalyst for 20 to 24 hours, or in pyridine in the presence of dicyclohexylcarbodiimide for one night to three days or in the presence of dimethylaminopyridine to obtain ##STR28##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04812512 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-5c112580e2254550a4c4f8214032cbe0 |
| Source note | uspto-grants-1989_03 |