Palmitic Acid → HCID 21269361, compound

HRID 1194275Notes

Reaction equation

HRID 1194275 reaction equation
[C:1]([OH:18])(=[O:17])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16].Cl[C:20]([O:22][CH2:23][CH3:24])=[O:21].C(=O)([O-])[O-].[Na+].[Na+]>C(Cl)Cl>[C:20](=[O:21])([O:22][CH2:23][CH3:24])[O:17][C:1](=[O:18])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

Participants

5

Reactant 3

HCID 985Palmitic AcidHCID 10340Sodium CarbonateHCID 10928Ethyl chloroformate

Product 1

HCID 21269361HCID 21269361, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

Palmitic acid and ethyl chloroformate are reacted with methylene chloride in a molar ratio of 1:1 in the presence of dry sodium carbonate. Inorganic material is filtered off, and the resulting filtrate is used directly in the reaction.

Workup

  1. filtrationInorganic material is filtered off
  2. customthe resulting filtrate is used directly in the reaction

Sources & evidence

ORD record
ord-5fe36ff0853d4b0fbe4e2bddd4a73543
Source dataset
uspto-grants-1989_03
Patent number
US04814112

Reaction notes

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