Potassium thiocyanate → HCID 14256955, compound

Participants

Reaction Steps

In 100 ml of formic acid, a reaction of 18.4 g of 5-chloro-2,4-diiodopyrimidine and 6.0 g of potassium thiocyanate was conducted at 60° C. for 1 hour in a similar manner as Synthesis Example 1. Then, the reaction mixture was treated in a similar procedure as Synthesis Example 1, there was obtained a 62.5% yield of 5-chloro-2-iodo-4-thiocyanopyrimidine, m.p. 183°-186° C.

Provenance & Evidence