HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54517743, compound → HCID 178419538, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54517743 | HCID 54517743 | — |
| Reactant | HCID 178513045 | HCID 178513045 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 178419538 | HCID 178419538 | — |
Reaction Steps
A mixture of 6.8 g. (0.02 mole) of N-n-hexyl-N- methyl-5-(2-bromoacetyl)furan-2-carboxamide, 2.4 g. (0.02 mole) of guanylthiourea and 225 ml. of acetone was stirred at room temperature for 2 hours. The solid was recovered by filtration (5.4 g.) and recrystallized from ethanol to give 812 mg. of the title compound as a white solid, mp. 226°-228° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04814341 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-bfaa9fd4d65c40e69266c4ba3349810a |
| Source note | uspto-grants-1989_03 |