HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-methyl-1-trityl-1H-imidazole-4-carbaldehyde → HCID 14520342, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-methyl-1-trityl-1H-imidazole-4-carbaldehyde | HCID 11824338 | — |
| Reactant | 8-bromo-6-chloro-2,2-dimethyl-4H-1,3-benzodioxin | HCID 14520336 | — |
| Product | HCID 14520342 | HCID 14520342 | 50% |
Reaction Steps
Starting from 8-bromo-6-chloro-2,2-dimethyl-4H-1,3-benzodioxin and 5-methyl-1-triphenylmethyl-1H-imidazole-4-carboxaldehyde. The addition of the organomagnesium compound is carried out at 0° C. Yield: 50% of theory;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04814343 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-12613cc0603c43bfb13a6d469555b9b6 |
| Source note | uspto-grants-1989_03 |