HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(triphenylmethyl)-1H-imidazole-4-carbaldehyde → HCID 14520345, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(triphenylmethyl)-1H-imidazole-4-carbaldehyde | HCID 618233 | — |
| Reactant | 6-Bromo-2,2-dimethyl-4H-benzo[d][1,3]dioxine | HCID 14520338 | — |
| Product | HCID 14520345 | HCID 14520345 | 54.5% |
Reaction Steps
Starting from 6-bromo-2,2-dimethyl-4H-1,3-benzodioxin and 1-triphenylmethyl-1H-imidazole-4-carboxaldehyde. The temperature of the reaction mixture does not exceed 40° C. Yield: 54.5% of theory; M.P.: 155°-162° C. (recrystallized from acetonitrile).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04814343 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-b1c06d966bc340c48388bad6b1527a8a |
| Source note | uspto-grants-1989_03 |