HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(triphenylmethyl)-1H-imidazole-4-carbaldehyde → HCID 14520346, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(triphenylmethyl)-1H-imidazole-4-carbaldehyde | HCID 618233 | — |
| Reactant | HCID 14520332 | HCID 14520332 | — |
| Product | HCID 14520346 | HCID 14520346 | 49.7% |
Reaction Steps
Starting from 1-bromo-2,6-dimethoxy-3-(1-methoxyethyl)benzene and 1-triphenylmethyl-1H-imidazole-4-carboxaldehyde. The reaction product is purified by chromatography on silica (eluent: 98:2 v/v dichloromethanemethanol). Yield: 49.7% of theory; M.P.: 96°-99° C. (recrystallized from acetonitrile).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04814343 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-10065241e72a411a9a2447b622975062 |
| Source note | uspto-grants-1989_03 |