HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(1-triphenylmethyl-1H-imidazol-4-yl)-1-pentanone → alpha-n-Butyl-alpha-(6-chloro-2,2-dimethyl-4H-1,3-benzodioxin-8-yl)-1-triphenylmethyl-1H-imidazole-4-methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(1-triphenylmethyl-1H-imidazol-4-yl)-1-pentanone | HCID 14520334 | — |
| Reactant | 8-bromo-6-chloro-2,2-dimethyl-4H-1,3-benzodioxin | HCID 14520336 | — |
| Product | alpha-n-Butyl-alpha-(6-chloro-2,2-dimethyl-4H-1,3-benzodioxin-8-yl)-1-triphenylmethyl-1H-imidazole-4-methanol | HCID 14520348 | 54.6% |
Reaction Steps
This compound is prepared like the preceding compound by reacting the organomagnesium compound of 8-bromo-6-chloro-2,2-dimethyl-4H-1,3-benzodioxin with 1-(1-triphenylmethyl-1H-imidazol-4-yl)-1-pentanone. Yield: 54.6% of theory; M.P.: 124° C. (recrystallized from petroleum ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04814343 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-7dc5d4e89dff43ec89611a727c9cff0f |
| Source note | uspto-grants-1989_03 |