HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21270012, compound → HCID 14520347, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21270012 | HCID 21270012 | — |
| Reactant | HCID 178418373 | HCID 178418373 | — |
| Product | HCID 14520347 | HCID 14520347 | 80% |
Reaction Steps
This compound is prepared like the preceding compound starting from methyl magnesium iodide and (6-chloro-2,2-dimethyl-4H-1,3-benzodioxin-8-yl)(1-triphenylmethyl-1H-imidazol-4-yl)ketone. The residue obtained after evaporation of the dichloromethane crystallizes when stirred in diethyl ether. Yield: 80% of theory; M.P.: 182°-184° C. (recrystallized from ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04814343 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-eb1ae821e27f469fa49170e7191da39d |
| Source note | uspto-grants-1989_03 |