Glycidol → HCID 86740360, compound

Participants

Reaction Conditions

Reaction Steps

Approximately 280 g of octadecylamine and about 0.35 liter of toluene were charged to a glass reactor and warmed to about 60° C. Over a 3 hour period of time, 38 g of glycidol were slowly added in small increments with agitation while maintaining a temperature of 60° to 65° C. The reactor contents were then heated at about 90° C. for 26 additional hours. The solvent was removed by vacuum distillation and the resulting product formed a pale yellow waxy solid after cooling.

Provenance & Evidence