HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 15686617, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-Azatricyclo(3.3.1.1,3,7)decan-4-one | HCID 142642 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 15686617 | HCID 15686617 | — |
Reaction Steps
A solution of 1-aza-adamantan-4-one (1.1 g), hydroxylamine hydrochloride (0.7 g) and pyridine (0.5 ml) in ethanol (30 ml) was heated under reflux for 1 h. The solution was then treated with saturated K2CO3 solution (30 ml), evaporated to half its volume and extracted with CH2Cl2 (4×50 ml). The combined extracts were dried (K2CO3) and evaporated in vacuo to give D.1 (1.2 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04816453 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-37121331cdb74b6fa7aeeec3e2d640ff |
| Source note | uspto-grants-1989_03 |