HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54131587, compound → HCID 21249120, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54131587 | HCID 54131587 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 21249120 | HCID 21249120 | — |
Reaction Steps
27.3 g (0.1 mole) of the compound obtained in Example 1 are dissolved in 200 ml of water and 15 ml of acetic acid. After addition of 15 g (0.23 mole) of zinc dust, the mixture is heated under reflux for 30 minutes and filtered. The aqueous phase is rendered alkaline and extracted, the extract is acidified and the resulting oil is separated off.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04816454 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-6f14db80a4de49f681bc80b8c9e44aef |
| Source note | uspto-grants-1989_03 |