HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 13592806, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 13592805 | HCID 13592805 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 13592806 | HCID 13592806 | — |
Reaction Steps
4 g (0.014 mole) of the compound prepared in Example 4 are stirred with 1 ml (0.021 mole) of hydrazine hydrate in 30 ml of ethanol and 20 ml of dimethylformamide at 80° C. for 2 hours. After the mixture has been cooled, the product is filtered off with suction and recrystallised from dimethylformamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04816454 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-78291319fe5747ccb845a78b046360aa |
| Source note | uspto-grants-1989_03 |