Hydrazine hydrate (1:1) → HCID 21249178, compound

HRID 1194670Notes

Reaction equation

HRID 1194670 reaction equation
[O:1]=[C:2]1[NH:6][CH2:5][CH:4]([C:7]2[CH:12]=[CH:11][C:10]([C:13](=O)[CH:14]([CH3:19])[CH2:15][C:16](O)=[O:17])=[C:9]([O:21][CH3:22])[CH:8]=2)[O:3]1.O.[NH2:24][NH2:25]>CO>[O:1]=[C:2]1[NH:6][CH2:5][CH:4]([C:7]2[CH:12]=[CH:11][C:10]([C:13]3[CH:14]([CH3:19])[CH2:15][C:16](=[O:17])[NH:24][N:25]=3)=[C:9]([O:21][CH3:22])[CH:8]=2)[O:3]1

Participants

4

Reactant 2

HCID 24654Hydrazine hydrate (1:1)HCID 21249154HCID 21249154, compound

Product 1

HCID 21249178HCID 21249178, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

5.9 g (0.019 mole) of 4-(4-(2-oxo-oxazolidin-5-yl)-methoxyphenyl)-4-oxo-3-methyl-butyric acid and 1.5 ml (0.031 mole) of hydrazine hydrate are heated under reflux in 30 ml of methanol for 1 hour.

Sources & evidence

ORD record
ord-fa410bcf65064fb0ba0d376950e3e55e
Source dataset
uspto-grants-1989_03
Patent number
US04816454

Reaction notes

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