HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21249173, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 21249125 | HCID 21249125 | — |
| Solvent | 2-Methoxyethanol | HCID 8019 | — |
| Product | HCID 21249173 | HCID 21249173 | — |
Reaction Steps
7.1 g (0.025 mole) of 4-(4-(3-pyridylmethyl)-phenyl)-4-oxo-3-methyl-butyric acid and 1.5 ml (0.03 mole) of hydrazine hydrate are stirred in 30 ml of ethylene glycol monomethyl ether at 100° C. for 1 hour. After addition of ethanolic hydrochloric acid, the product is filtered off with suction and recrystallised from 96% strength ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04816454 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-8c7cf0a6d30b4dd388505b6cb9464c58 |
| Source note | uspto-grants-1989_03 |