HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → HCID 15631970, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | HCID 12273863 | HCID 12273863 | — |
| Product | HCID 15631970 | HCID 15631970 | — |
Reaction Steps
A mixture of the compound of Example 6 (5.0 g, 0.018 mol) and phenol (3.38 g, 0.036 mol) is reacted as described for Example 14 to obtain the free base which is recrystallized three times from hexane to afford the title compound as a crystalline solid, m.p. 182°-184° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04816464 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-e70e45a11e9b4837893c32da822881c3 |
| Source note | uspto-grants-1989_03 |