HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → HCID 12233753, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | Aniline | HCID 6115 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 12273863 | HCID 12273863 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 12233753 | HCID 12233753 | — |
Reaction Steps
By the method described for Example 14, a mixture of the compound of Example 6 (15.0 g, 0.0562 mol), 10.69 (0.115 mol) of phenol and 10.3 mol (0.115 mol) of aniline is reacted. Thereafter, the reaction mixture is slurried with a mixture of 10% aqueous potassium hydroxide and diethyl ether. The insoluble product is filtered and recrystallized from acetonitrile giving the title compound (13.0 g, 72%), m.p. 137°-139° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04816464 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-e018674de04e44a68d1324a258213ec8 |
| Source note | uspto-grants-1989_03 |