HCID 13286104, compound → HCID 13286105, compound

HRID 1194758Notes

Reaction equation

HRID 1194758 reaction equation
[CH:1]1([NH:7][S:8]([CH2:11][C:12]2[CH:17]=[CH:16][C:15]([N+:18]([O-])=O)=[CH:14][CH:13]=2)(=[O:10])=[O:9])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1>C(O)(C)C>[NH2:18][C:15]1[CH:16]=[CH:17][C:12]([CH2:11][S:8]([NH:7][CH:1]2[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6]2)(=[O:10])=[O:9])=[CH:13][CH:14]=1

Participants

3

Reactant 1

HCID 13286104HCID 13286104, compound

Product 1

HCID 13286105HCID 13286105, compoundYield 86.9%

Reagents, catalysts & solvents 1

HCID 3776IsopropanolSolvent

Procedure

By a procedure similar to that described in example 9(b) the product of stage (a) (6.4 g) was hydrogenated to give the title compound (5.0 g), m.p. 141°-143° (from isopropanol).

Sources & evidence

ORD record
ord-04d3dd91a6264a49b5c94ecfac4a5b25
Source dataset
uspto-grants-1989_03
Patent number
US04816470

Reaction notes

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