HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methoxyacetyl chloride → HCID 136336892, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methoxyacetyl chloride | HCID 96623 | — |
| Reactant | HCID 136336893 | HCID 136336893 | — |
| Product | HCID 136336892 | HCID 136336892 | — |
Reaction Steps
Reaction of hydrated 9-(1,3-dihydroxy-2-propoxymethyl)guanine (1 mmole) with methoxyacetyl chloride (4 mmole) according to the method used for 9-[1,3-bis(phenoxyacetoxy)-2-propoxymethyl]guanine (Example 14) gives, after chromatography, the desired product. Confirmation of structure and purity are obtained by NMR and TLC (9:1CHCl3 --MeOH).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04816447 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-1403ea548bdc4cad988f3e156e27e9c5 |
| Source note | uspto-grants-1989_03 |