1-Bromodecane → HCID 86742842, compound

Participants

Reaction Steps

20.8 g (0.1 Mol) of 2,4-dihydroxycaprophenone together with 32 g (0.145 Mol) of n-decylbromide and 14 g of anhydrous potassium carbonate in 150 ml of dried acetone, as in Example 11, were converted to ketone, between 45° C. and 47° C. in flash point, which, in absence of potassium acetate, reacted with hydroxylamine hydrochloride in ethanolic solution to oxime, 57° C. in flash point (ethanol/water).

Provenance & Evidence