1-Bromooctane → HCID 86742843, compound

Participants

Reaction Steps

29.2 g (0.1 Mol) of 2,4-dihydroxylaurophenone together with 28 g (0.145 Mol) of n-octylbromide and 14 g of anhydrous potassium carbonate in 150 ml of dried acetone, as in Example 11, are converted to ketone, 56° C. to 57° C. in flash point (ethanol), and, subsequently, with hydroxylamine hydrochloride in the presence of potassium acetate in ethanolic solution, converted to oxime, between 60° C. and 63° C. in flash point (ethanol, n-heptane). The following example was obtained in the same way: 4-decyloxy-2-hydroxy-laurophenone-oxime, between 64° C. and 69° C. in flash point (n-heptane, ethanol).

Provenance & Evidence