HRID1194882

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID16992

Cycloheptane, bromo-

C7H13Br

$结构：CCOC(=O)/C(=N\O)C(C)=O$

HCID178472876

未命名化合物

PRODUCTS

生成物

$结构：CCOC(=O)/C(=N\OC1CCCCCC1)C(C)=O$

HCID14864956

未命名化合物

收率 80%

PROCEDURE

实验过程

Ethyl (Z)-2-(hydroxyimino)-3-oxobutyrate (5.Og) was treated with cycloheptyl bromide as described in Example 13a to give the title compound as a colourless liquid (6.36 g, 80%). (Found: M+ +H, 256.1547, C13H21NO4 requires M+H 256.1550), νmax (film) 2940, 1750, 1690 cm-1 ; δH (CDCl3): 1.31 (3H, t) 1.4-2.0 (12H, m), 2.35 (3H, s) 4.32 (3H, q+m).