cis-2-Methylcyclohexanol → HCID 140352839, compound

Participants

Reaction Steps

Ethvl (Z)-2-hydroxyimino-3-oxobutyrate (1.59 g) was alkylated with cis-2-methylcyclohexan-1-ol (1.71 g) as described in Example 4, method 3. The pure title compound was otained as a pale yellow oil (0.506 g). (Found: M+, 256.1552. C13H21NO4 requires M 256.1549); νmax (film) 1745, 1695 and 1595 cm-1 ; δH (CDCl3) 1.02 (3H, d, J 6 Hz), 1.35 (3H, t, J 7 Hz), ca 1.2-2.3 (9H, m), 2.40 (3H, s), 3.95 (1H, m) and 4.42 (2H, q, J 7 Hz).

Provenance & Evidence