HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178453393, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 178453395 | HCID 178453395 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178453393 | HCID 178453393 | — |
Reaction Steps
Into 75 ml of MeOH was dissolved 8.9 g (10.4 mmoles) of Z-D-Lys(BOC)-Phe-Arg-CHA.HCl. After adding 1 gram of palladium black, it was catalytically reduced at 30° C. for 8 hours. After the reaction, the catalyst was filtered off and the solvent was distilled off under reduced pressure. Thus, 6.4 g (85.3%; a foamed product) of H-D-Lys(BOC)-Phe-Arg-CHA.2HCl was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04816562 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-f9f7e2a047154ffcb5b5958a8ea5f8f2 |
| Source note | uspto-grants-1989_03 |