HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1194993Generated: October 26, 2026
Isopropanol → Isopropylphosphite Triethylammonium
https://huagongshe.com/reaction/1194993
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Phosphorous acid, bis(1-methylethyl) ester | HCID 21884976 | — |
| Solvent | Water | HCID 962 | — |
| Product | Isopropylphosphite Triethylammonium | HCID 88392515 | 95% |
Reaction Steps
Diisopropylphosphite (10.0 g, 0.06 moles), triethylamine (14.6 g, 0.14 moles), isopropanol (20 ml), and water (10 ml) were mixed in a flask under an argon atmosphere and heated at 60° C. for 48 hours. The volatile components were removed under vacuum, leaving a viscous, clear oil. The resulting product was produced in 95% yield (12.8 g) and had the following spectral data:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04816571 |
|---|
| Source dataset | uspto-grants-1989_03 |
|---|
| ORD ID | ord-a068d83c59e2488aacfde75b285df7f9 |
|---|
| Source note | uspto-grants-1989_03 |
|---|
