反应详情

温度

60 °C

Diisopropylphosphite (10.0 g, 0.06 moles), triethylamine (14.6 g, 0.14 moles), isopropanol (20 ml), and water (10 ml) were mixed in a flask under an argon atmosphere and heated at 60° C. for 48 hours. The volatile components were removed under vacuum, leaving a viscous, clear oil. The resulting product was produced in 95% yield (12.8 g) and had the following spectral data:

1. customThe volatile components were removed under vacuum
2. customleaving a viscous, clear oil
3. customThe resulting product was produced in 95% yield (12.8 g)