HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diglyme → HCID 21269152, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diglyme | HCID 8150 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 12330044 | HCID 12330044 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 21269152 | HCID 21269152 | — |
Reaction Steps
A mixture of 6.0 g. of sodium borohydride, 26 ml. of diglyme, 14 ml. of water, and 4.8 g. of methyl 6,11-dihydro-11-bromodibenz[b,e]oxepin-2-acetate is heated at 50° for one hour. Water is added and the mixture is extracted with ether. The ether extracts are dried with sodium sulfate, filtered, and concentrated in vacuo to provide methyl 6,11-dihydrodibenz[b,e]oxepin-2-acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04816591 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-47a0cd5bac0b4c1a8e7ce00791539aaf |
| Source note | uspto-grants-1989_03 |