HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 14848847, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4-(5-Decylpyrimidin-2-yl)benzoic acid | HCID 14645819 | — |
| Product | HCID 14848847 | HCID 14848847 | 99.6% |
Reaction Steps
4-(5-n-Decyl-2-pyrimidyl)benzoic acid (2.0 g) prepared in the above (3) was added to thionyl chloride (10 g) and a slight amount of N,N-dimethylformaide was added thereto and the mixture was refluxed for 4 hours. Excess thionyl chloride was distilled off to obtain the titled compound (2.1 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05110496 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-7efde1339a594cc7b6e9bb0976ea960e |
| Source note | uspto-grants-1992_05 |