Sodium Bicarbonate → HCID 135487736, compound

HRID 1195126Notes

Reaction equation

HRID 1195126 reaction equation
[NH2:1][C@H:2]([C:7]([NH:9][C@H:10]([C:15]([OH:17])=[O:16])[CH2:11][CH2:12][S:13][CH3:14])=[O:8])[CH2:3][CH:4]([CH3:6])[CH3:5].[C:18](=[O:21])(O)[O-:19].[Na+].Cl.[NH:24]1[C:32](=[O:33])[C:31]2[NH:30][CH:29]=[N:28][C:27]=2[N:26]=[CH:25]1>O.C1(C)C=CC=CC=1>[NH:24]1[C:32](=[O:33])[C:31]2[N:30]=[CH:29][N:28]([CH2:7][CH2:2][CH2:3][CH2:4][CH2:5][O:19][C:18]([NH:1][C@H:2]([C:7]([NH:9][C@H:10]([C:15]([OH:17])=[O:16])[CH2:11][CH2:12][S:13][CH3:14])=[O:8])[CH2:3][CH:4]([CH3:6])[CH3:5])=[O:21])[C:27]=2[N:26]=[CH:25]1

Participants

6

Reactant 3

HCID 516892Sodium BicarbonateHCID 701052936077-39-1HCID 135724455HCID 135724455, compound

Product 1

HCID 135487736HCID 135487736, compound

Reagents, catalysts & solvents 2

HCID 962WaterSolventHCID 1140TolueneSolvent

Procedure

0.850 g (0.0032 mole) of leucyl-methionine and 0.824 g (0.0096 mole) of sodium bicarbonate were dissolved in 40 ml of bidistilled water, in a 150 ml flask. To the resulting aqueous solution, having pH=8, a suspension of 1.05 g (0.0032 mole) of 9-[5-chlorocarbonyloxy)pentyl]hypoxanthine hydrochloride in 40 ml of toluene was added in ice bath.

Workup

  1. additionwas added in ice bath

Sources & evidence

ORD record
ord-61778444060647879e7f499bbe21f47e
Source dataset
uspto-grants-1992_05
Patent number
US05110798

Reaction notes

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