HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 54067527, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Ethyl 3-bromopropionate | HCID 68320 | — |
| Reactant | HCID 13530069 | HCID 13530069 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 54067527 | HCID 54067527 | — |
Reaction Steps
26.1 g (0.1 mol) of 4,4-di(p-fluorophenyl)butylamine and 18.1 g of 3-bromopropionic acid ethyl ester are refluxed with 21.0 g of potassium carbonate in 200 ml of 2-butanone for 24 hours while stirring. The reaction mixture is filtered and the filtrate is concentrated by evaporation under reduced pressure, yielding crude 3-[4,4-di(p-fluorophenyl)-butylamino]-propionic acid ethyl ester in the form of an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05110807 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-4c2e0af4cd0d47ff8297408e9d49868b |
| Source note | uspto-grants-1992_05 |