HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1195238Generated: November 2, 2026
HCID 19819017, compound → HCID 19819020, compound
https://huagongshe.com/reaction/1195238
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 19819017 | HCID 19819017 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 19819020 | HCID 19819020 | 55% |
Reaction Steps
A solution of dicyclopropylmethanimine hydrochloride (1.00 g, 6.87 mmol) in 6.0 ml of dimethyl sulfoxide was heated with stirring at 100° C. for 4 hours. The solvent was distilled out in vacuo and isobutyl alcohol (6 ml) was added to the residue. Precipitated crystals was obtained and dried in vacuo to afford 0.55 g (Yield: 55%) of the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05110945 |
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| Source dataset | uspto-grants-1992_05 |
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| ORD ID | ord-d0db1dab158242feb1f62fa127826663 |
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| Source note | uspto-grants-1992_05 |
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