Methylamine → HCID 19001654, compound

HRID 1195319Notes

Reaction equation

HRID 1195319 reaction equation
[O:1]1[C:5]2[CH:6]=[CH:7][C:8]([CH:10]([S:14][CH2:15][C:16]([OH:18])=O)[CH2:11][CH2:12][CH3:13])=[CH:9][C:4]=2[O:3][CH2:2]1.[CH3:19][NH2:20]>>[CH3:19][NH:20][C:16](=[O:18])[CH2:15][S:14][CH:10]([C:8]1[CH:7]=[CH:6][C:5]2[O:1][CH2:2][O:3][C:4]=2[CH:9]=1)[CH2:11][CH2:12][CH3:13]

Participants

3

Reactant 2

HCID 6329MethylamineHCID 14514901HCID 14514901, compound

Product 1

HCID 19001654HCID 19001654, compound

Procedure

2.5 g of the title compound was prepared from 2.7 g of [{1-(1,3-benzodioxol-5-yl)butyl}thio]acetic acid by using a 40% aqueous solution of methylamine as a colorless oil according to the same procedure as that described in Example 27.

Sources & evidence

ORD record
ord-e29ca8c98f1443c2b6c0e8a5795a4bf6
Source dataset
uspto-grants-1992_05
Patent number
US05110956

Reaction notes

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