HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 53975244, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 24904076 | HCID 24904076 | — |
| Product | HCID 53975244 | HCID 53975244 | — |
Reaction Steps
In a manner analogous to that described in Example 2 it is also possible, by reacting 2-chloro-9-(2-fluorobenzyl)-9H-purine (Example 7) with N-methylamine, to obtain the 9-(2-fluorobenzyl)-2-(N-methylamino)-9H-purine, which has a melting range of from 184° to 185° (methanol/diethyl ether), the reaction mixture being heated for 24 hours at from 80° to 85°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05110818 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-414d419ea0c241fe8bdccf3f2a684ba3 |
| Source note | uspto-grants-1992_05 |