HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 14832336, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 14832328 | HCID 14832328 | — |
| Catalyst | Dimethylformamide | HCID 6228 | — |
| Product | HCID 14832336 | HCID 14832336 | — |
Reaction Steps
9.7 g (0.02 mol) of 2-(4-carboxyphenyl)-2-[4-(4-nitrophenoxy)phenyl]hexafluoropropane were suspended in 47 cm3 of thionyl chloride, a few drops of dimethylformamide were added, and the mixture was refluxed until evolution of gas was no longer observed. The thionyl chloride was removed by distillation, and the residue was recrystallized from acetonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05110983 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-de1705453aa645babb12665ed84d4b41 |
| Source note | uspto-grants-1992_05 |