HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 14857377, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 14857308 | HCID 14857308 | — |
| Solvent | tert-Butanol | HCID 6386 | — |
| Product | HCID 14857377 | HCID 14857377 | — |
Reaction Steps
A mixture of 5.8 g of 2,2-dimethyl-4-(1-benzyl-1,2-dihydro-2-oxo-3-pyridyl)-6-cyano-3-chromanol, 11.6 g of KOH and 90 ml of tert.-butanol is boiled for 50 min., cooled and poured onto ice. Customary working up gives 2,2-dimethyl-4-(1-benzyl-1,2-dihydro-2-oxo-3-pyridyl)-6carbamoyl-3-chromene, m.p. 199°-202°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05112839 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-552ff9e1d5f640d09a830f2c9b3b37a7 |
| Source note | uspto-grants-1992_05 |