HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → HCID 14857385, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 14857381 | HCID 14857381 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 14857385 | HCID 14857385 | — |
Reaction Steps
A mixture of 2.98 g of 2,2-dimethyl-4-(1,2-dihydro-2-oxo-3-pyridyl)-6-carbamoylchroman,2 ml of POCl3 and 200 ml of 1,2-dichloroethane is boiled for 45 min. Cooling and customary working up gives 2,2-dimethyl-4-(1,2-dihydro-2-oxo-3-pyridyl)-6-cyanochroman, m.p. 174°-175.5°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05112839 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-e8ef9b70feeb4a3aba38700d4231d5f8 |
| Source note | uspto-grants-1992_05 |