HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl Peroxide → HCID 14368704, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 14368703 | HCID 14368703 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 14368704 | HCID 14368704 | — |
Reaction Steps
1.35 g of 5,7-Difluoro-1-methylnaphthaline in 10 ml of carbon tetrachloride are refluxed for 41/2 hours with 1.4 g of N-bromosuccinimide and 50 mg of dibenzoylperoxide. The cooled mixture is filtered and the solvent removed under vacuum. The purity of the crystalline crude product is sufficient for further reaction, m.p. 74°-76.5°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05112851 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-8c79336066a24a918e8010e041886d60 |
| Source note | uspto-grants-1992_05 |