HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodine → HCID 53739951, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodine | HCID 807 | — |
| Reactant | Diiodomethane | HCID 6346 | — |
| Reactant | HCID 54481297 | HCID 54481297 | — |
| Catalyst | Copper | HCID 23978 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 53739951 | HCID 53739951 | — |
Reaction Steps
600 mg of Copper powder are cauterized with 10 mg of iodine in 10 ml of toluene. 1.2 g of Diiodomethane and 500 mg of 1-(4-cyanophenyl)-1-(4-chlorophenyl)-ethylene are added and the mixture refluxed for 140 hours and then filtered and the filtrate concentrated. The oily residue is chromatographed on silica gel with toluene as eluant.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05112851 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-cb5f4a7023b642f0ac9b743926db2342 |
| Source note | uspto-grants-1992_05 |