HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → HCID 53883034, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 53739951 | HCID 53739951 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 53883034 | HCID 53883034 | — |
Reaction Steps
230 mg of Lithiumaluminiumhydride are suspended in 10 ml of tetrahydrofuran, 234 mg of 1-(4-chlorophenyl)-1-(4-cyanophenyl)cyclopropane in 5 ml tetrahydrofuran added dropwise and the mixture refluxed for 18 hours. The mixture is then hydrolysed with 1N HCl and extracted with dichloromethane. The oily title compound is directly reacted further.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05112851 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-a553eb9a2897465f91a8ba39c908d69f |
| Source note | uspto-grants-1992_05 |