HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → N-Benzyl-3,4-diacetoxy-5-nitrobenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | 2,6-Lutidine | HCID 7937 | — |
| Reactant | 3,4-Diacetoxy-5-nitrobenzoic acid | HCID 15480740 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | N-Benzyl-3,4-diacetoxy-5-nitrobenzamide | HCID 19389240 | — |
Reaction Steps
0.75 g of 3,4-diacetoxy-5-nitrobenzoic acid was converted to the corresponding acid chloride as described in Example 43. It was dissolved in 5 ml of dichloromethane and added to a solution containing 0.27 ml of benzylamine and 0.5 ml of 2,6-lutidine in 7 ml of dichloromethane. Yield 0.95 g (96%), a viscous oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05112861 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-16eb610541ab4098a555406227938881 |
| Source note | uspto-grants-1992_05 |