Ethylene Glycol → 2-(tetrahydrofuran-2-yl)-1,3-dioxolane

HRID 1196082Notes

Reaction equation

[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH:6]=[O:7].[CH2:8](O)[CH2:9][OH:10]>>[O:1]1[CH2:5][CH2:4][CH2:3][CH:2]1[CH:6]1[O:10][CH2:9][CH2:8][O:7]1

Participants

Reactant 2

HCID 174Ethylene Glycol

HCID 7362Furfural

Product 1

HCID 2631622-(tetrahydrofuran-2-yl)-1,3-dioxolane

Procedure

Note: 2-(2-oxolanyl)-dioxolane was prepared in similar manner by reacting 2-furaldehyde and ethylene glycol and then hydrogenating the reaction product. The product characterization was confirmed by I. R., 1 H nmr and 13 C nmr.

Sources & evidence

ORD record: ord-931c0b014c2b4259bcaac64c893a9ae7
Source dataset: uspto-grants-1992_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05112929

Reaction notes

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