Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1196165Generated: November 2, 2026

HCID 19938212, compound → N-methylcyclohexanecarboxamide

https://huagongshe.com/reaction/1196165

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 19938212HCID 19938212—
SolventHydrochloric AcidHCID 313—
SolventEthyl AcetateHCID 8857—
ProductN-methylcyclohexanecarboxamideHCID 334382750.7%

Reaction Steps

In 50 ml of ethyl acetate saturated with hydrogen chloride was dissolved 2.18 g of compound 137 obtained by Example 137, and the solution was stirred for 1 hour. Thereafter, the solvent was evaporated under reduced pressure, and the residue was recrystallized from methanol to afford 0.31 g of the desired compound (Compound 138).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05112867
Source datasetuspto-grants-1992_05
ORD IDord-3d788a5b39fd4ffba4fd3e042f0e2bd2
Source noteuspto-grants-1992_05