HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19938212, compound → N-methylcyclohexanecarboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19938212 | HCID 19938212 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | N-methylcyclohexanecarboxamide | HCID 3343827 | 50.7% |
Reaction Steps
In 50 ml of ethyl acetate saturated with hydrogen chloride was dissolved 2.18 g of compound 137 obtained by Example 137, and the solution was stirred for 1 hour. Thereafter, the solvent was evaporated under reduced pressure, and the residue was recrystallized from methanol to afford 0.31 g of the desired compound (Compound 138).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05112867 |
| Source dataset | uspto-grants-1992_05 |
| ORD ID | ord-3d788a5b39fd4ffba4fd3e042f0e2bd2 |
| Source note | uspto-grants-1992_05 |